Unambiguous NMR spectral assignments of salvinorin A.
نویسندگان
چکیده
The complete assignments of the (1)H and (13)C NMR spectra of the hallucinogenic neoclerodane diterpenoid salvinorin A were determined in three different NMR solvents using HSQC, HMBC and COSY. Solvent systems are described that allow the resolution of all (1)H signals. Virtual coupling was observed for the protons at C-2, C-3 and C-4 in the 600 MHz (1)H spectrum in CDCl(3). The complete assignments of the (1)H and (13)C NMR spectra of salvinorin B are also reported.
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ورودعنوان ژورنال:
- Magnetic resonance in chemistry : MRC
دوره 45 4 شماره
صفحات -
تاریخ انتشار 2007